|
Laboratory of Optical Spectroscopy
(ECD, ORD, VCD, UV-VIS-NIR, IR)
Head: Prof. Jadwiga Frelek
phone (022) 343 22 15, jadwiga.frelek@icho.edu.pl
ELECTRONIC CIRCULAR DICHROISM SPECTROSCOPY (ECD)
Analytical capabilities
- Electronic circular dichroism measurements in solution, in nujol or in a solid state (KCl, KBr or CsI pellets) within the 163 nm to 1100 nm spectral range;
-
Solid-state measurements in reflectance and transmittance circular dichroism
(DRCD/DTCD) mode;
-
Measurements of fluorescence detected circular dichroism (FDCD) at the
constant temperature within the -10 °C to +110 °C temperature range with an
accuracy of ± 0.1 °C;
-
Titration measurement with the ECD/UV-VIS and fluorescence detection
(at the constant temperature);
-
Linear dichroism spectroscopy (LD);
-
HPLC separations with ECD (or OR) and UV-VIS (or RI) detection;
- Measurements within the 50 °C to -196 °C temperature range, with ±0.1 °C stability and accuracy;
- Measurements within the 25 °C to 250 °C temperature range, with ±1 °C stability and accuracy;
- ECD kinetics measurements at the constant temperature within pre-assigned spectral range or at the selected wavelength.
Equipment
- Spectropolarimeter ECD Jasco J-715;
- Spectropolarimeter ECD Jasco J-815, for solid state measurements;
-
Peltier Cell Holder with Fluorescence Capability (-10 °C to 110 °C temperature
range w/accuracy up to ±0.1 °C);
-
Automatic Titrator;
-
Cryostat Optistat, Oxford Instruments (-196 °C to 50 °C temperature range
w/accuracy up to ±0.1 °C);
-
Thermostat Specac (25 °C to 250 °C temperature range w/accuracy up ±1 °C);
-
Recirculating thermostat Julabo (-88 °C to 100 °C temperature range w/accuracy
up ±0.1 °C).
 Request for analysis
[Pricing]
OPTICAL ROTATORY DISPERSION (ORD)
Analytical capabilities
- Optical rotatory dispersion measurements in solution within the 185 nm to
700 nm spectral range at the constant temperature;
- Measurements within
the -10 °C to 110 °C temperature range, with ±0.1 °C stability and accuracy;
-
ORD kinetics measurements at the constant temperature within pre-assigned
spectral range or at the selected wavelength.
Equipment
- Spectropolarimeter ORD Jasco J-815
Request for analysis
[Pricing]
VIBRATIONAL CIRCULAR DICHROISM (VCD)
Analytical capabilities
- Vibrational circular dichroism measurments in solution within the 4000 nm to
850 cm-1
spectral range;
- Mesurment in solid-state (KBr/KCl pellet), in nujol mull or
in form of a solution-deposited thin-film using rotating holder (SyncRoCell);
-
Temperature measurement in aqueous solution within the -4 °C to +80 °C
temperature range, with ±0.1 °C stability and accuracy.
Equipment
-
ChiralIR-2X
TM
DualPEM
BioTools spectrometer
Request for analysis
[Pricing]
ULTRAVIOLET-VISIBLE AND NEAR-INFRARED SPECTROSCOPY (UV-VIS-NIR)
Analytical capabilities
- Qualitative and quantitative measurements within 190 to 2700 nm (standard 190-900 nm) spectral range in solution, in nujol and in solid state (KCl, KBr or CsI pellet);
- Measurements for solid state (powder, paste, thin film) and liquid samples, using integrating sphere attachement for both the
diffuse-transmitted or diffuse-reflected light;
- UV-VIS-NIR spectral measurements of kinetics within a defined spectral range or at a defined wavelength.
Equipment
- Spectrophotometer UV-VIS-NIR Jasco V-670 (190-2700 nm spectral range);
- Spectrophotometer UV-VIS Carry 100E (190-900 nm spectral range).
Request for analysis
[Pricing]
INFRARED SPECTROSCOPY (IR)
Analytical capabilities
- Qualitative and quantitative IR spectroscopy in 7800 to 350 cm-1 (standard 4000-400 cm-1)
spectral range for samples in form of a solution-deposited thin-film, a liquid
thin-film, a solution (IR cell), a nujol mull or KBr pellet.
- Reflectance IR spectroscopy for liquid or solid samples using ATR accessory with diamond or zinc selenide crystal.
Equipment
- Spectrophotometer FTIR Jasco 6200;
- Spectrophotometer FTIR Spectrum 2000 Perkin Elmer.
Request for analysis
[Pricing]
We offer also a possibility to carry out a non-standard measurements at Client's request after prior case-by-case consultation with our analytical staff. The analytical reports are delivered as a hard-copy printouts and/or as a computer files, in format acceptable to our Clients (such as txt, rtf, pdf or doc).
|
|
 |
